图书简介
A practical guide to ICP emission spectrometry, updated with information on the latest developments and applications The revised and updated third edition of ICP Emission Spectrometry contains all the essential information needed for successful ICP OES analyses. In addition, the third edition reflects the most recent developments and applications in the field. Filled with illustrative examples and written in a user-friendly style, the book contains material on the instrumentation instructions on how to develop effective methods. Throughout the text, the author-a noted expert on the topic-incorporates typical questions and problems and provides checklists and detailed instructions for implementation. The third edition includes 10 new chapters that cover recent progress in both the application and methodology of the technology. New information on plasma, the optics, and the detector of the spectrometer is also highlighted. This revised third edition: Contains fresh chapters on the newest developments Presents several new chapters on plasma as well as the optics and the detector of the spectrometer Offers a helpful troubleshooting guide as well as examples of practical applications Includes myriad illustrative examples Written for lab technicians, students, environmental chemists, water chemists, soil chemists, soil scientists, geochemists, and materials scientists, ICP Emission Spectrometry, Third Edition continues to offer the basics for successful ICP OES analyses and has been updated with the latest developments and applications.
OVERVIEW Analytic features of the ICP OES ICP OES - definitions Distribution of the ICP emission spectrometers Complimentary techniques for elemental analysis MIP and LIPS Symbols, abbreviations and acronyms used PLASMA The analytically used plasma Argon Added gases (e.g. Oxygen or Nitrogen) Materials used for ICP torches Orientation of the plasma (e.g. vertical vs. horizontal) Excitation to emit electromagnetic radiation High-frequency generator Sample introduction system Nebulizers OPTICS AND DETECTOR OF THE SPECTROMETER Principles of optics Detector Emission spectrometer mounts Scanning Array Spectrometers Simultaneous Array Spectrometers METHOD DEVELOPMENT Wavelength selection Reference to NIST-Atlas Processing and correction techniques Non-spectral interferences Optimization Validation Procedure to check linearity ROUTINE ANALYSIS Preliminary steps Calibration Quality control Software and data management TROUBLE SHOOTING APPLICATIONS General Notes Notes on specific elements Selected applications INSTRUMENT PURCHASING AND LABORATORY PREPARATION Which technique in atomic spectrometry is preferred? Which ICP emission spectrometer is best for the application? Preparation of the laboratory LITERATURE INDEX
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